碳氫化合物取本品作為供試品;取甲烷含量為0.0020%的氣體(以氮氣為稀釋劑)作為對照氣體,照氣相色譜法(通則0521)試驗,用玻璃球為填料的色譜柱(0.8m×4mm,80目);柱溫為110℃;進樣口溫度為110℃;檢測器溫度為120℃。量取供試品氣體與對照氣體,注入氣相色譜儀,在凈化溫度為360℃時測得的峰面積為相應(yīng)空白值;量取供試品氣體與對照氣體,注入氣相色譜儀,測定峰面積,減去相應(yīng)空白值后的峰面積為校正峰面積。按外標法以校正峰面積計算,含碳氫化合物(以甲烷計)不得過0.0020%。
浩瀚色譜研制生產(chǎn)的玻璃球柱包括轉(zhuǎn)接頭,密封墊等,輕松的安裝在安捷倫7820A,7890B,8860,8890,6890,HP4890,HP5890,柱效高,峰型對稱,分析時間短,效率高。滿足2020年版藥典二氧化碳中碳氫化合物的檢測要求。
色譜柱實現(xiàn)互聯(lián)互通,填充柱/毛細管柱進樣口,均可安裝,使用簡單,方便,快捷。
名稱:填充柱
固定相:玻璃球
粒度:80目
規(guī)格:0.8m*4mm
型號:HH-BLQ
應(yīng)用:藥典2020年版二氧化碳中碳氫化合物的分析
Take this product as the test sample for hydrocarbons; Take a gas with a methane content of 0.0020% (using nitrogen as the diluent) as the control gas, and perform gas chromatography (General Rule 0521) according to the test. Use a glass ball packed chromatographic column (0.8m x 4mm, 80 mesh); The column temperature is 110 ℃; The inlet temperature is 110 ℃; The detector temperature is 120 ℃. Measure the gas of the test sample and the control gas, inject them into the gas chromatograph, and the peak area measured at a purification temperature of 360 ℃ is the corresponding blank value; Measure the gas of the test sample and the control gas, inject them into the gas chromatograph, measure the peak area, and subtract the corresponding blank value to obtain the corrected peak area. According to the external standard method for correcting peak area, the content of hydrocarbons (calculated as methane) shall not exceed 0.0020%.
The glass ball columns developed and produced by Haohan Chromatography include adapters, sealing gaskets, etc., which can be easily installed on Agilent 7820A, 7890B, 886088906890, HP4890, HP5890, with high column efficiency, symmetrical peak shapes, short analysis time, and high efficiency. Meet the detection requirements for hydrocarbons in carbon dioxide in the 2020 edition of the Pharmacopoeia.
The chromatographic columns are interconnected, and both the filling column and capillary column injection ports can be installed, making them simple, convenient, and fast to use.
Name: Filled Column
Fixed phase: glass ball
Particle size: 80 mesh
Specification: 0.8m * 4mm
Model: HH-BLQ
Application: Analysis of hydrocarbons in carbon dioxide in Pharmacopoeia 2020 edition