1、從氨和甲醇催化合成甲胺時(shí),首先制備甲醇和氨的汽化混合物,接下來(lái)在反應(yīng)器中,在大約220℃-約500℃、大氣壓-約50巴的壓力下,通過(guò)使其從催化劑床上經(jīng)過(guò)而進(jìn)行反應(yīng)。
2、氨和甲醇的反應(yīng)產(chǎn)物為三種胺(一甲胺、二甲胺、三甲胺)的混合物,以及水、氨和未反應(yīng)的甲醇組成。
3、在這些產(chǎn)物中,一甲胺是工業(yè)上最希望得到的一種胺,其作為原料可用作醫(yī)藥、農(nóng)藥(西維因、樂(lè)果、殺蟲(chóng)脒等),染料(茜素中間體、蒽醌系中間體等),及燃料(水膠藥、一甲肼等),表面活性劑、促進(jìn)劑、以及橡膠助劑、 照相化學(xué)品和溶劑等。
GB/T 30303-2013 工業(yè)用甲胺和甲胺水溶液試驗(yàn)方法
范圍
本標(biāo)準(zhǔn)規(guī)定了工業(yè)用甲胺和甲胺水溶液的試驗(yàn)方法。
本標(biāo)準(zhǔn)適用于甲醇連續(xù)氣相催化氨化生產(chǎn)的一甲胺、二甲胺、三甲胺及其配制的水溶液的測(cè)定
名稱:填充柱
型號(hào):GDX-103:四乙烯戊胺:氫氧化鉀 =90:9:1
規(guī)格:3m*3mm,60-80目
*高使用溫度:120°C
編號(hào):20240625002
適用于安捷倫,島津,賽默飛,瓦里安,布魯克,PE,北分瑞利,東西電子,華愛(ài),上分,科創(chuàng),天瑞,天美,科曉*捷島,福立,川儀,魯南瑞虹等
分析:甲胺及甲胺類水溶液
1. When catalyzing the synthesis of methylamine from ammonia and methanol, a vaporized mixture of methanol and ammonia is first prepared. Then, in the reactor, the reaction is carried out by passing it through the catalyst bed at a pressure of about 220 ℃ - about 500 ℃ and atmospheric pressure - about 50 bar.
2. The reaction product of ammonia and methanol is a mixture of three amines (monomethylamine, dimethylamine, trimethylamine), as well as water, ammonia, and unreacted methanol.
3. Among these products, monomethylamine is the most desired amine in industry. As a raw material, it can be used in medicine, pesticides (such as carbapenem, dimethoate, chlorpyrifos, etc.), dyes (such as alizarin intermediates, anthraquinone intermediates, etc.), fuels (such as hydrogels, monomethylhydrazine, etc.), surfactants, promoters, rubber auxiliaries, photographic chemicals, and solvents.
GB/T 30303-2013 Test Methods for Methylamine and Methylamine Aqueous Solutions for Industrial Use
Range
This standard specifies the test methods for industrial methylamine and methylamine aqueous solutions.
This standard is applicable to the determination of monomethylamine, dimethylamine, trimethylamine and their prepared aqueous solutions in the continuous gas-phase catalytic amination production of methanol
Name: Filled Column
Model: GDX-103: Tetraethylpentamine: Potassium hydroxide=90:9:1
Specification: 3m * 3mm, 60-80 mesh
*High operating temperature: 120 ° C
Number: 20240625002
Applicable to Agilent, Shimadzu, Thermo Fisher, Varian, Brooke, PE, Kitafen Ruili, Dongxi Electronics, Huaai, Uesugi, Sci Tech Innovation, Tianrui, Tianmei, Kexiao * Jiedao, Fuli, Chuanyi, Lunan Ruihong, etc
Analysis: Methylamine and methylamine aqueous solutions